Observation and reactivity of the chainlike species ([Al(PO4)2](super -3))n during the X-ray diffraction investigation of the hydrothermal synthesis of the super-sodalite sodium aluminophosphate MIL-74 (Na2Al7(PO4)12.4trenH3.Na(H2O)16)

Article Abstract:

A study of the hydrothermal synthesis of the aluminum phosphate Na2Al7(PO4)12.4trenH3.Na(H2O)16(MIL-74) is presented by X-ray diffraction and in-situ time-resolved energy-dispersive X-ray diffraction. The observation of an intermediate phase in the study allows for the proposition of a chemical reaction pathway for the formation of the three-dimensional network of MIL-74.

All Other Basic Inorganic Chemical Manufacturing, Industrial inorganic chemicals, not elsewhere classified, Potassium & Sodium Compounds, Sodium & Sodium Compounds, Aluminum Compounds, Usage, Phosphates, X-rays, X-ray diffraction, Sodium compounds

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Cation exchange, dehydration, and calcination in clinoptilolite: in situ X-ray diffraction and computer modeling

Article Abstract:

The dehydration and cation mobility in Clinoptilolite using in situ synchroton dispersion and microcrystal diffraction using a hybrid simulation technique is studied. The result shows the "heat collapse" framework transformation with the help of in situ diffraction data and computer modeling.

Science & research, Research, Analysis, Synchrotron, Synchrotrons, Chemistry, Physical and theoretical, Physical chemistry, Dehydration (Chemical process), Heat exhaustion

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• Abstracts: An in situ energy-dispersive x-ray diffraction study of the hydrothermal crystallization of zeolite A. 1. Influence of reaction conditions and transformation into sodalite. part 2

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